期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 133, 期 3, 页码 428-429出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja1099853
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资金
- Japan Science and Technology Agency, JST [22000008]
- Global COE Program for Chemistry Innovation
- University of Tokyo ASATSU-DK China
Coupling of an alkyl chloride with a secondary benzamide derivative at the ortho-position can be achieved in good to excellent yield in the presence of a cobalt catalyst and cyclohexylmagnesium chloride in diethyl ether at room temperature. Cyclohexylmagnesium chloride formally acts to remove hydrogen atoms from the amide nitrogen and from the ortho-position and to generate the active cobalt species.
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