期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 134, 期 1, 页码 7-10出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja210959p
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资金
- Welch Foundation [E-1571]
- National Institute of General Medical Sciences [R01GM077635]
- A. P. Sloan Foundation
- Camille and Henry Dreyfus Foundation
A method for five- and six-membered heterocycle formation by palladium-catalyzed C-H/N-H coupling is presented. The method employs a picolinamide directing group, PhI(OAc)(2) oxidant, and toluene solvent at 80-120 degrees C. Cyclization is effective for sp(2) as well as aliphatic and benzylic sp(3) C-H bonds.
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