期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 130, 期 49, 页码 16807-16811出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja806304s
关键词
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资金
- SRC/ERC program of MOST/KOSEF [R11-2007-107-02001-0]
- National Research Foundation of Korea [과06A1501, R11-2007-107-02001-0] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
The first asymmetric total synthesis of (-)-laurefucin (1), a unique C-15 acetogenin with a 2,8-dioxabicyclo[5.2.1]decane skeleton, has been accomplished in nine steps in 31% overall yield from known oxocene 10. Highlights of the highly stereoselective synthesis include a novel organoselenium-mediated biomimetic hydroxyetherification.
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