期刊
JOURNAL OF SYNCHROTRON RADIATION
卷 19, 期 -, 页码 705-709出版社
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S0909049512029640
关键词
Fresnel zone plate; hard X-rays; full-field transmission X-ray microscopy; solid-oxide fuel cell
资金
- US DOE [DE-AC02-06CH11357]
- Energy Frontier Research Center on Science Based Nano-Structure Design and Synthesis of Heterogeneous Functional Materials for Energy Systems (HeteroFoaM Center)
- US Department of Energy, Office of Science, Office of Basic Energy Sciences [DE-SC0001061]
Full-field transmission X-ray microscopy is a unique non-destructive technique for three-dimensional imaging of specimens at the nanometer scale. Here, the use of zone-doubled Fresnel zone plates to achieve a spatial resolution better than 20 nm in the hard X-ray regime (8-10 keV) is reported. By obtaining a tomographic reconstruction of a Ni/YSZ solid-oxide fuel cell, the feasibility of performing three-dimensional imaging of scientifically relevant samples using such high-spatial-resolution Fresnel zone plates is demonstrated.
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