4.6 Article

Nanosized TiO2 particles decorated on SiO2 spheres (TiO2/SiO2): synthesis and photocatalytic activities

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出版社

SPRINGER
DOI: 10.1007/s10971-010-2272-z

关键词

Nanosized TiO2/SiO2; Sol-gel; TiO2 photocatalyst; SiO2 core shell; Methylene blue degradation

资金

  1. Prince of Songkla University
  2. NSF Science and Technology Center of Advanced Materials for Purification of Water with Systems (Water CAMPWS)
  3. U.S. Department of Energy [DEFG02-91-ER45439]

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Nanosized TiO2 and nano-anatase TiO2 decorated on SiO2 spherical core shells were synthesized by using a sol-gel method. The synthesized pure TiO2 nano particle and TiO2 grafted on SiO2 sphere with various ratios have been characterized for their structure and morphologies by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Fourier transform infrared spectrophotometry (FTIR) and transmission electron microscopy (TEM). Their surface areas were measured using the BET method. The photocatalytic activity of all nanocomposites was investigated using methylene blue as a model pollutant. The synthesized TiO2/SiO2 particles appeared to be more efficient in the degradation of methylene blue pollutant, as compared to pure TiO2 particles.

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