期刊
JOURNAL OF SEPARATION SCIENCE
卷 34, 期 1, 页码 107-112出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.201000583
关键词
Ion mobility spectrometry; Molecular imprinted polymer; Testosterone
资金
- Research Council of Isfahan University of Technology
Analysis of testosterone was accomplished using corona discharge ion mobility spectrometry. Molecular imprinted polymer was used for the extraction and pre-concentration of testosterone. Analytical parameters including precision, dynamic range and detection limit were obtained. The linear dynamic range was from 10 to 250 ng/mL and the limit of detection was 0.9 ng/mL. The proposed method was used for analysis of testosterone in urine samples. A urine sample from a 3-year-old girl was used as the blank. The RSD was below 10%. The obtained results from the method were also compared with the standard method for analysis of testosterone using SPE-HPLC analysis. The results demonstrate the accuracy of the method.
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