期刊
JOURNAL OF RARE EARTHS
卷 31, 期 5, 页码 449-455出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/S1002-0721(12)60302-0
关键词
yttrium orthophospha; sacrificial template; europium; lithium; photoluminescence; hollow microspheres; rare earths
资金
- Shanxi Provincial Science and Technology Plan Foundation of China [20110321037-02]
Li+ and Eu3+ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene (PS) as template. Techniques of X-ray diffraction (XRD), scanning electron microscopy (SEM), as well as transmission electron microscopy (TEM) were employed to characterize the as-synthesized sample. Furthermore, the photoluminescence (PL) characterization of the Li+ and Eu3+ co-doped YPO4 microsphere was carried out and the effects of the doping concentration of Li+ and Eu3+ active center concentration as well as calcination temperature on the PL properties were studied in detail. The results showed that the incorporation of Li+ ions into the YPO4:Eu3+ lattice could induce a remarkable improvement of the PL intensity. The highest emission intensity was observed with the compound of 5%Li+ and 5%Eu3+ co-doped YPO4, whose brightness was increased by a factor of more than 2.2 in comparison with that of the YPO4:5%Eu3+.
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