期刊
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
卷 301, 期 1, 页码 263-268出版社
SPRINGER
DOI: 10.1007/s10967-014-3132-z
关键词
Uranium; Chromotrope 2R; Ionic liquid based micro-extraction; Multivariate determination; UV-Vis spectrophotometry
资金
- Scientific and Technological Research Council of Turkey (TUBITAK) under 2216 Research Fellowship Programme for Foreign Citizens''
A simple, fast and reliable spectrophotometric method for the determination and microextraction of trace amounts of uranium using chromotrope 2R as a chelating agent and 1-butyl-3-methylimidazolium hexafluorophosphate ionic liquid (IL) was used as an extractant solvent. Influence variables such as pH, volume of ligand and IL were inspected by full factorial design. In the view of Pareto chart a contour plot was studied to examine the significant variables and their interactions. The detection limit and the preconcentration factor were found to be 0.87 and 50 mu g L-1, respectively. The developed method was successfully applied to ore samples.
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