期刊
JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY
卷 46, 期 13, 页码 4556-4563出版社
WILEY
DOI: 10.1002/pola.22792
关键词
conducting polymers; conjugated polymers; polycondensation
Zero-valent palladium complex, Pd(PTh3)(3), with three tri(2-thienyl)phosphine ligands was prepared and characterized. Pd(PTh3)(3) is superior to Pd(PPh3)(4) in catalyzing Suzuki-Miyaura coupling and polymerization of thiophene-based derivatives. The Suzuki polycondensation of 3-hexyl-5-iodothiophene-2-boronic pinacol ester with Pd(PTh3)(3) as the catalyst precursor afforded high-molecular-weight P3HT with high regularity and yield. (C) 2008 Wiley Periodicals, Inc.
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