期刊
JOURNAL OF PHYSICS D-APPLIED PHYSICS
卷 45, 期 43, 页码 -出版社
IOP PUBLISHING LTD
DOI: 10.1088/0022-3727/45/43/435303
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资金
- Shandong Province Middle-aged and Young Scientists Research Incentive Fund [BS2009CL016]
- Fundamental Research Funds for the Central Universities [201113002]
The nucleation and growth kinetics of the formation of water-soluble CdSe quantum dots (QDs) was characterized by measurements of their optical properties of ultraviolet-visible and fluorescence spectra. The QDs were synthesized using thioglycolic acid as a capping agent. Two kinetic parameters, reaction temperature and time, were varied over wide ranges 20-90 degrees C and 0-12 h, respectively. Our results showed that a low reaction temperature was preferable for the nucleation process, resulting in relatively small particles and a narrow size distribution. The subsequent grain growth was mainly achieved within 1 h. The reaction temperature virtually affected the kinetic features of the QDs. The fluorescence measurements revealed largest variations of the fluorescence features for the 70 degrees C samples. From a viewpoint of controls of fluorescence colour and intensity over a wide range, a reaction temperature of 70 degrees C was appropriate for the CdSe QD synthesis.
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