期刊
JOURNAL OF PHYSICAL CHEMISTRY C
卷 116, 期 8, 页码 5055-5061出版社
AMER CHEMICAL SOC
DOI: 10.1021/jp300745g
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资金
- DOE [DE-FG02-90ER4S429]
- Ministero dell'Istruzione, Universita e della Ricerca Scientifica (MIUR) [prot. 20087K9A2J]
- Consorzio Interuniversitario per lo Sviluppo dei Sistemi a Grande Interfase (CSGI)
The basic building block of calcium-silicate-hydrate (C-S-H) gel, which is the major hydration product of a commercial Portland cement paste, is usually referred as globule in the Jennings' colloidal model-II developed for C-S-H. The detailed nanostructure of the globule is so far not given quantitatively. In this paper, we determine the structural parameters of the building block with good accuracy by small-angle neutron scattering technique probing an extended interval of the scattering vector, Q from 0.015-1.0 angstrom(-1). In this Q-range an interlamellar peak at 0.65-0.80 angstrom(-1) is present, shifting as a function of the water content present in the C-S-H gel. This additional feature enables us to confirm the presence of a lamellar structure and determine the thicknesses of both the water and the hydrated calcium silicate layers respectively proper of the C-S-H globules.
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