期刊
JOURNAL OF PHYSICAL CHEMISTRY C
卷 113, 期 13, 页码 5031-5034出版社
AMER CHEMICAL SOC
DOI: 10.1021/jp810492s
关键词
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资金
- Institute of Nuclear Energy Research
- Atomic Energy Council, Taiwan [NL94025 I]
- National Science Council [NSC94-2113-M-009-012, 94-2120-M-009-014]
Zr-doped ceria nanotuhes (ZrxCe1-xO2) Were obtained in a high yield from a hydrothermal reaction in an aqueous solution of NaOH with Ce(NO3)(3)center dot 6H(2)O and ZrO2 powder in a small proportion. The morphology and crystalline structure were characterized with X-ray diffraction, a scanning electron microscope, and a transmission electron microscope. Mechanisms for the growth of Zr-doped ceria nanotubes are proposed based oil the Kirkendall effect, the formation of the tubular structure is strongly dependent oil the precursor. This is the first report of a direct synthesis of cerium-oxide nanotubes in high yield. The surface area of the nanotubes is 76 m/g and their average pore size is similar to 52.2 nm, Catalytic measurements show that the nanotubes as synthesized are active for an oxygen-storage capacity and for ethanol reforming.
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