期刊
JOURNAL OF PHYSICAL CHEMISTRY C
卷 113, 期 16, 页码 6566-6572出版社
AMER CHEMICAL SOC
DOI: 10.1021/jp9005718
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资金
- National Key Project of Fundamental Research [2005CB6236-05]
- National Natural Science Foundation of China [50672112]
- Hundred Talent Program
In this paper, we report a facile method to prepare high-yield one dimensional hierarchical beta-Co(OH)(2) nanocolumns through one-step hydrothermal synthesis with hydrazine hydrate and Na3PO4 as morphology-directing agents, which play important roles in the formation of hierarchical nanocolumn morphology. The hierarchical Co3O4 nanocolumns are obtained by the beta-Co(OH)(2) nanocolumns annealed at 400 degrees C for 4 h. The formation mechanism of hierarchical nanocolumns has been clearly demonstrated by studying morphology evolution processes of beta-Co(OH)(2) nanocrystals upon reaction time, which undergo two steps, the formation of nanorods and then growing sideways in the form of thin nanoplatelets to form hierarchical nanocolumns. Moreover the UV-vis spectra and magnetic properties Of Co3O4 nanocolumns also have been investigated.
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