期刊
JOURNAL OF PHYSICAL CHEMISTRY B
卷 112, 期 46, 页码 14461-14469出版社
AMER CHEMICAL SOC
DOI: 10.1021/jp802879a
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资金
- Innovation Fund of Science and Research (Hungary)
- General Secretariat for Research and Technology (Greece)
Loading of graphite oxide (GO) with tris(2,2'-bipyridyl) iron(II) ions and subsequent calcination affords a novel graphene-based composite with magnetic and electrically conductive properties. The pH of the starting-aqueous suspension and the washing procedure play a crucial role in the Successful immobilization of the iron precursor, which is mainly governed by ion exchange. The complex is intercalated between the graphene oxide layers, where it adopts a distorted conformation. Rapid heating of this solid results ill the deflagration of GO and the formation of ultrafine (d = 2-14 nm) Fe2O3 particles with maghemite as the dominant phase. The superparamagnetic maghemite crystals are dispersed uniformly in the high-surface-area diamagnetic matrix built up from single or turbostratic stacked graphenes.
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