期刊
JOURNAL OF ORGANOMETALLIC CHEMISTRY
卷 693, 期 21-22, 页码 3425-3429出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jorganchem.2008.08.007
关键词
cyclotetramerization; metallophthalocyanine; synthesis; microwave; 1,2,4-triazole
资金
- Karadeniz Technical University, Trabzon, Turkey
The synthesis of metallophthalocyanines [6-9; M = Ni(II), Zn(II), Co(II) and Cu(II)] with four 1,2,4-triazole units obtained from 4-{(4-chloro-2-fluorobenzyl)[3-(4-chlorophenyl)-5-(4-methylphenyl)-4H-1,2,4-triazol-4-yl] amino} phthalonitrile (5) in the presence of dimethylaminoethanol and the corresponding anhydrous metal salts is described. The thermal stabilities of the Pc compounds were determined by thermogravimetric analysis. The new compounds were characterized by a combination of IR, H-1 NMR, C-13 NMR, UV-Vis, elemental analysis. (C) 2008 Elsevier B.V. All rights reserved.
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