期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 83, 期 17, 页码 9707-9717出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.8b01210
关键词
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资金
- Russian Scientific Foundation [14-50-00069]
- Russian Science Foundation [14-50-00069] Funding Source: Russian Science Foundation
The hydrolytic imidazoline ring expansion (HIRE) methodology was extended to readily available tetracyclic [1,4]thiazepines as well as sulfoxide and sulfone analogs thereof. The reactions resulted in the facile formation of a rare medium-sized [1,4,7]thiazecine ring system that has an emerging utility in bioactive compound design. Comparing the HIRE rates for representative compounds in the three groups of substrates allowed drawing some generalizations about the substituent effects on the course of the reaction.
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