期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 79, 期 5, 页码 2296-2302出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo500019a
关键词
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资金
- National Natural Science Foundation of China [21232003, 21202053, 21272087]
- National Basic Research Program of China [2011CB808603]
A [3 + 2] cycloaddition/ring contraction sequence of ylideneoxindoles with in situ-generated 2,2,2-trifluorodiazoethane without the use of any transition-metal catalyst has been developed. The reaction provides efficient access to biologically important and synthetically useful CF3-containing 3,3'-cyclopropyl spirooxindoles in high yield (74-99%) with high diastereoselectivity (>95:5 d.r.).
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