期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 78, 期 10, 页码 5045-5050出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo400244h
关键词
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A new method of CuCN-mediated one-pot cyclization of 4-(2-bromophenyl)-2-butenoates leading to efficient synthesis of substituted naphthalene amino esters including phenanthrene aromatic structural units is described. Deuterium labeling studies establish that this one-pot cascade cyclization proceeds through isomerization of olefin, intramolecular C-C bond cyclization, and aromatization as the key intermediates, all occurring in a single step.
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