期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 78, 期 17, 页码 8442-8450出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo401165y
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资金
- Department of Science and Technology, New Delhi [JCB/SR/S2/JCB-26/2010]
- CSIR, New Delhi
- University Grants Commission
A reagent system comprising tetrabutylammonium nitrate-trifluoroacetic anhydride-triethylamine has been developed for the synthesis of 2-nitroglycals from various protected glycals. The base-catalyzed Ferrier rearrangement on tri-O-acetylated 2-nitroglycals has been reported for the first time. Reactivity of these nitroacetates and associated selectivity has been examined, and some of the products have been converted into 2,3-diamino-2,3-dideoxyglycosides and methyl N-acetyl-b-lividosaminide.
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