期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 77, 期 17, 页码 7640-7645出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo301001j
关键词
-
资金
- Ministero dell'Istruzione, dell'Universita e della Ricerca (MIUR, Rome, Italy) [2008A7P7YJ]
- European Commission
- FSE (Fondo Sociale Europeo)
- Calabria Region
A novel approach to 3-iodothiophenes by direct iodocyclization of alkynylthiol derivatives is presented. A variety of 1-mercapto-3-yn-2-ols 5 (readily available from alkynylation of the corresponding alpha-mercapto ketones or alpha-mercapto esters) were smoothly converted into the corresponding 3-iodothiophene derivatives 6 in good yields by reaction with molecular iodine in the presence of NaHCO3 at room temperature in MeCN as the solvent.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据