期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 75, 期 4, 页码 1301-1304出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo902533p
关键词
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资金
- Danish Natural Science Research Council
- Danish Medical Research Council
- The Danish Council for Independent Research/Technology and Production Sciences [09-070364]
A protocol for rapid and efficient Pd/Cu-catalyzed coupling of aryl bromides and iodides to terminal alkynes has been developed with use of 2-(di-tert-butylphosphino)-N-phenylindole (cataCXium PIntB) as ligand in TMEDA and water. The new protocol successfully couples substrates which failed with standard Sonogashira conditions, and enables an efficient general synthetic route to free fatty acid 1 (FFA1) receptor ligands from 3-(4-bromophenyl)-propionic acid.
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