期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 74, 期 8, 页码 3172-3174出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo900205x
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资金
- Italian Ministero dell'Istruzione, dell'Universit e della Ricerca [2006030948002]
An efficient synthesis of 3-substituted crotonaldehydes via alkyne-enol ether cross-metathesis in the presence of CuSO4 and in aqueous medium was developed. Crotonaldehydes were obtained in good yields from terminal aryl-alkynes as well as from terminal alkyl-alkynes. All of the reactions were carried out under microwave irradiation and were completed in a few minutes. Water was used as the cosolvent, making c, this approach safer, economic, and desiderable from an enviromental point of view.
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