期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 74, 期 3, 页码 1341-1344出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo802355d
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资金
- NDSEG
- NSF [547905]
- Amgen
- AstraZeneca
- Boehringer Ingelheim
- DuPont
- GlaxoSmithKline
- Lilly
Electrophilic activation of secondary amides with trifluoromethanesulfonic anhydride in the presence of 2-fluoropyridine followed by introduction of a pyridine N-oxide derivative and warming affords the corresponding N-pyridinyl tertiary amide derivatives. A mechanism supported by in situ monitoring and deuterium labeling experiments is discussed.
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