期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 74, 期 15, 页码 5559-5561出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo9009112
关键词
-
资金
- NIH [1R01-AT59000-01A1]
A formal total synthesis of the antitubercular natural product was accomplished. This work was undertaken to address certain stereochemical problems in our initial synthesis. By using an ester group as a surrogate for a methyl group, we were able to intercept a key intermediate in our first synthesis with better selectivity and greater convergence than had previously been the case.
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