期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 74, 期 1, 页码 254-263出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo8018285
关键词
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资金
- Australian Research Council [ARC-DP0665068]
- Australian Postgraduate Award
- Australian Government
A fast and efficient route for diversity-oriented synthesis of 3- and 2,3-disubstituted piperidines, featuring an intramolecular nitrone cycloaddition with high regio- and diastereoselectivity, was achieved in six steps and 36-66% overall yield from commercially available gamma-butyrolactone or 1,4-butanediol. A new N-alkenyl nitrone enoate was used in this intramolecular nitrone cycloaddition, and the regioselectivity, diastereoselectivity, and reversibility of this cycloaddition were investigated.
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