期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 73, 期 7, 页码 2768-2773出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo702694g
关键词
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资金
- NIGMS NIH HHS [R01 GM043854-11, GM-43854, R01 GM043854-12, R01 GM043854-13, R01 GM043854-10, R01 GM043854, R01 GM043854-14] Funding Source: Medline
ent-Cholesterol was synthesized in 16 steps,from commercially available (S)-citronellol. The overall yield for the synthesis was 2.0%. This route is amenable to gram-scale preparation of ent-cholesterol. Isotopic incorporation near the end of the synthesis was achieved using labeled methyl iodide. This synthesis is the most practical to date and will make ent-cholesterol more readily available to use as a probe of the function and metabolism of cholesterol.
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