期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 73, 期 8, 页码 3063-3069出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo702455g
关键词
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Syntheses of the four enantionterically pure diastereoisomers of the phytoprostanes E(1) type II and 15-E(2t)-isoprostanes (1-4) are described. The key steps included the preparation of the Freimanis (+/-)-hydroxycyclopentenone 5, enzymatic resolution of this racemic hydroxycyclopentenone, Wittig and Horner-Wadsworth-Emmons (HWE) coupling reactions and finally enantioselective reductions.
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