期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 73, 期 14, 页码 5574-5577出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo800461r
关键词
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N-Benzylhexahomotriaza-p-chlorocalix[3]trinaphthylamide in partial cone conformation was selectively synthesized by appropriately controlling the steric effect during the amidation reactions of N-benzylhexahomotriaza-p-chlorocalix[3]tri-(ethyl acetate) in cone or partial cone conformations with use of 1-aminomethylnaphthalene. The conformation was confirmed by H-1, C-13, and D-2 NMR and X-ray single-crystal analysis. Analyses of the complexes revealed that recognition is strongly affected by Cd2+, Pb2+, and F- ions.
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