期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 73, 期 2, 页码 745-748出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo7018703
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[GRAPHICS] An efficient and high-yielding approach for the asymmetric synthesis of calcimimetic (+)-NPS R-568 (1) has been developed. The key step of the synthesis is the highly diastereoselective addition of methyl Grignard to the (S-S,E)-N-(3-methoxybenzylidene)-2-propanesulfinamide [5(S)], which afforded a single diastereoisomer in high yield in short reaction time.
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