期刊
JOURNAL OF NANOPARTICLE RESEARCH
卷 14, 期 7, 页码 -出版社
SPRINGER
DOI: 10.1007/s11051-012-0982-6
关键词
Nickel-phthalocyanine; Solid-phase pyrolysis; Nickel nanoparticles; Carbon nanostructures; Magnetic properties
资金
- International Innovative Nanotechnology Center (ININC) CIS [10881]
- ANSEF [PS-CONDMATEX-1199]
- Republic of Armenia [65]
By using a modified method of solid-phase pyrolysis of metal-phthalocyanines, we have synthesized ferromagnetic Ni nanoparticles in different carbon structures: amorphous carbon plates, multiwall carbon nanotubes, carbon fibers, and graphitized capsules. The composition, structure and morphology of prepared composite materials have been studied by energy dispersive X-ray microanalysis, scanning and transmission electron microscopy, and X-ray diffraction technique. It has been found that the sizes of nickel nanoparticles (10-500 nm) and the type of carbon structures strongly depend on the pyrolysis conditions. By using the X-band ferromagnetic resonance measurements, we have revealed features of the temperature dependence of resonance spectra of single-domain and multi-domain Ni nanoparticles in Ni/C composites.
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