4.6 Article

Recrystallization, texture evolution, and magnetostriction behavior of rolled (Fe81Ga19)98B2 sheets during low-to-high temperature heat treatments

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JOURNAL OF MATERIALS SCIENCE
卷 49, 期 13, 页码 4565-4575

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SPRINGER
DOI: 10.1007/s10853-014-8156-9

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资金

  1. National Basic Research Program of China (973 Program) [2012CB619404]
  2. National Natural Science Foundation of China [51101006, 51221163, 50925101]

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In order to study the texture evolution and magnetostriction behavior in the rolled Fe-Ga-B sheets during the heat treatments from low to high temperatures, (Fe81Ga19)(98)B-2 sheets were prepared and investigated. The phase structure, recrystallization, grain size, texture evolution, and magnetostriction behavior during the annealing from 525 to 1200 A degrees C for 1-5 h were investigated using X-ray diffraction, electron backscattering diffraction, and standard strain-gauge measurements. Results indicated that the primary recrystallization temperature for 1-h annealing was found as 525-575 A degrees C in (Fe81Ga19)(98)B-2 sheets. Annealing the sample below 575 A degrees C for 1 h, the release of rolling stress and increase of aOE (c) 100 > eta-fiber texture during the primary recrystallization jointly resulted in a rapid improvement in magnetostriction. After annealed between 575 and 1100 A degrees C for 1 h, the grains of the sheets underwent a normal growth, and the three (alpha-, gamma- and eta-fiber) types of textures kept an approximate balance, leading to a plateau of magnetostriction around 75 ppm. When the abnormal grain growth proceeded above 1100 A degrees C for 1 h, the proportion of eta-fiber texture markedly increased, and the magnetostriction was subsequently increased to 97 ppm. For longer annealing durations, the strong ideal cube texture (eta-fiber) was firstly formed and then changed to undesired texture (gamma-fiber), producing a corresponding magnetostriction peak of 136 ppm at 2 h for the annealing at 1200 A degrees C. The clear correlation among heat treatments, recrystallization, texture, and magnetostriction provides an essential understanding for Fe-Ga-B alloy sheets.

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