期刊
JOURNAL OF MATERIALS CHEMISTRY
卷 19, 期 32, 页码 5850-5854出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/b908214j
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资金
- DTRA [HDTRA1-07-1-0024]
- NSF [CHE0315275]
- ONR [N00014-06-1-1032]
The nitrogen-rich energetic material 3,4,5-triamino-1-tetrazolyl-1,2,4-triazole (TATT) was synthesized from diaminoguanidine using a straightforward method. The assumption that a 1,2,4-triazole ring is an intermediate in the one-pot reaction is supported by the synthesis of TATT from an analogous reaction of 3,4,5-triamino-1,2,4-triazole with cyanogen azide. TATT center dot HNO3 crystallizes in the monoclinic system P21/c. TATT has excellent thermal stability which resembles triaminotrinitrobenzene (TATB), but with a higher positive heat of formation and greater impact insensitivity.
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