期刊
JOURNAL OF MAGNETIC RESONANCE
卷 198, 期 2, 页码 275-281出版社
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jmr.2009.02.012
关键词
C-13 direct detection; Protonless NMR; Intrinsically disordered proteins; Virtual decoupling; IPAP; Spin-state selection
资金
- EC [026145, 031220]
- Ente Cassa di Risparmio di Firenze
Here, we present a series of exclusively heteronuclear multidimensional NMR experiments, based on C-13 direct detection, which exploit the H-1 polarization as a starting source to increase the signal-to-noise ratio. This contributes to make this spectroscopy more useful and usable. Examples are reported for a suitable system such as securin, an intrinsically disordered protein of 22 kDa. (C) 2009 Elsevier Inc. All rights reserved.
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