4.3 Article

Synthesis and Characterization of Novel Poly-thiophene-nanoporous Silica and its Application for Mercury Removal from Waste Waters

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TAYLOR & FRANCIS INC
DOI: 10.1080/10601325.2013.735955

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Modified nanoporous silica; poly-thiophene; mercury removal; waste waters

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In this work, MCM-41 (Mobil Composition of Matter number 41) nanoporous silica has been synthesized and characterized by X-ray powder diffraction and IR spectroscopy. In the next step, poly-thiophene was coated on the nanoporous silica in order to increase its surface area. This composite was characterized by X-Ray powder diffraction, High resolution transmission electronic microscopy micrograph (HRTEM), elemental analysis (CHNS) and Thermal analysis (TG/DTA). The application of this composite was investigated in mercury ions removal from waste water prior to determination by inductively coupled plasma atomic emission spectroscopy (ICP-OES). In order to investigate the effect of nanoporous structure on the efficiency of this composite, the same composite without porous structure has been synthesized and the results were compared.

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