期刊
ORGANIC LETTERS
卷 17, 期 5, 页码 1204-1207出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b00155
关键词
-
资金
- Welch Foundation [E-1571, Chair E-0044]
- NIGMS [R01GM077635]
- University of Houston
A method for aminoquinoline-directed, cobalt-promoted dimerization of benzamides has been developed. Reactions proceed in ethanol solvent in the presence of Mn(OAc)(2) cocatalyst and Na2CO3 base and use oxygen as a terminal oxidant. Bromo, iodo, nitro, ether, and ester moieties are compatible with the reaction conditions. Cross-coupling of electronically dissimilar aminoquinoline benzamides proceeds with modest yields and selectivities.
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