期刊
ORGANIC LETTERS
卷 17, 期 20, 页码 4984-4987出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b02426
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资金
- MEXT/JSPS KAKENHI [25288016]
- Asahi Glass Foundation
- Izumi Science and Technology Foundation
- Grants-in-Aid for Scientific Research [26870079, 25288016] Funding Source: KAKEN
Dibenzo[g,p]chrysenes were readily synthesized via the superacid- or TiF4-mediated domino Friedel-Crafts-type cyclization of 1,1-difluoroethenes bearing two biaryl groups, which were easily prepared via the Suzuki-Miyaura coupling of 1,1-difluoro-2,2-diiodoethene or 1-(biphenyl-2-yl)-1-bromo-2,2-difluoroethene. Using this approach, the activation of both vinylic and aromatic C-F bonds was successfully achieved to make new C-C bonds.
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