期刊
ORGANIC LETTERS
卷 17, 期 5, 页码 1264-1267出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b00246
关键词
-
资金
- Ministry of Science and Technology of the Republic of China [NSC 102-2113-M-037-005-MY2]
A novel Bi(OTf)(3)-mediated cycloisomerization of gamma-alkynyl arylketones 4, 7, or 10 with molecular sieve (MS) in MeNO2 affords 3-substituted furans 3, 8, or 11 at rt for 3 h in moderate to good yields. The method provides mild, less-toxic, atom-economic and efficient conditions. The mechanism has been studied and proposed. Moreover, this route can be enlarged to gram scale.
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