期刊
ORGANIC LETTERS
卷 17, 期 23, 页码 5776-5779出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b02992
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资金
- NIH [GM104180]
- Ford Foundation
- Eli Lilly
- Novartis
- Bristol-Myers Squibb
- Amgen
- Boehringer-Ingelheim
- Sloan Foundation
- Baxter Foundation
Dissection of lepadiformine by a double hydroamination transform affords a simple achiral amino diene. This reaction is accomplished in the forward sense by amine-directed hydroboration and an oxidative alkyl shift to nitrogen, both of which occur with high stereoselectivity to generate three stereogenic centers and the lepadiformine skeleton.
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