期刊
ORGANIC LETTERS
卷 17, 期 16, 页码 4050-4053出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b01970
关键词
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资金
- National Science and Technology Major Projects of China [2014ZX10005002-005]
- Foundation of Key Laboratory of Plant Resources Conservation and Sustainable Utilization (South China Botanical Garden, Chinese Academy of Sciences)
A remarkable TFA-mediated method for the construction of a biologically interesting tricyclic ketal skeleton was uncovered by starting from a variety of readily available acylphloroglucinol and diacylphloroglucinol substrates. This approach, which mimics a biosynthetic olefin isomerization/hemiacetalization/dehydration/(3 + 3) type cycloaddition sequence through a 2H-furan-1-ium intermediate, establishes a viable synthetic strategy for efficient synthesis of bullataketals analogs.
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