期刊
ORGANIC LETTERS
卷 17, 期 17, 页码 4396-4399出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b02380
关键词
-
资金
- DFG [SFB749]
- FRQNT
Functionalized 4-benzylated pyridines can be efficiently prepared by a transition-metal-free cross-coupling between various benzylic zinc chlorides and substituted 4-cyanopyridines in THF/DMPU under microwave irradiation (40 degrees C, 0.5-1.5 h). Selective benzylations on polycyano-aromatics have also been achieved under these mild conditions. We also report a novel oxidative nudeophilic substitution of a hydrogen on 1,3-dicyanobenzene using benzylic zinc reagents.
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