期刊
ORGANIC LETTERS
卷 17, 期 10, 页码 2298-2301出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b00422
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资金
- Center for Drug Discovery at Georgetown University Medical Center
The facile total synthesis of the natural product (+/-)-mahanine was obtained in eight steps with an overall 52% yield from readily accessible known nitrophenol derivative 6. After a one-step, acid-catalyzed annulation, two additional natural products were formed including 7-hydroxymurrayazolinine, representing its first reported total synthesis. In the whole process, the introduction of the m-nitro group significantly enhanced the key pyran annulation reaction through inductive effects.
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