期刊
ORGANIC LETTERS
卷 17, 期 9, 页码 2126-2129出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b00716
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资金
- NIGMS CMLD initiative [P50 GM067041]
- Boston University Undergraduate Research Opportunities Program (UROP)
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1156666] Funding Source: National Science Foundation
Cyclization of 1,6-diynes promoted by stoichiometric Ga(III) halides produces vinyl halides in good to excellent yields. Under acidic conditions, initially formed iodocyclization products undergo in situ Friedel-Crafts cyclizations, giving access to iodoindenopyridines. Application of the vinyl halides in cross-coupling reactions has been explored, and mechanistic aspects of the cyclization are discussed.
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