期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 13, 期 18, 页码 5105-5109出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ob00632e
关键词
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资金
- USTC Research Fund
- Nanyang Technological University
- Singapore Ministry of Education Academic Research Fund [ETRP 1002 111, MOE 2010-T2-2-067, MOE 2011-T2-1-013]
The Fe-III-or Ag-I-catalyzed oxidative fluorination of cyclopropanols via radical rearrangement is disclosed. This process features a straightforward and highly effective protocol for the site-specific synthesis of beta-fluoroketones and represents an expedient method for the synthesis of gamma-, delta- and epsilon-fluoroketones. Notably, this reaction proceeds at room temperature and tolerates a diverse array of cyclopropanols.
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