4.6 Article

Metal-free oxysulfenylation of alkenes with 1-(arylthio)pyrrolidine-2,5-diones and alcohols

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ORGANIC & BIOMOLECULAR CHEMISTRY
卷 13, 期 17, 页码 4846-4850

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ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ob00252d

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  1. National Natural Science Foundation of China [21172128, 21372139, 21221062]
  2. Ministry of Science and Technology of China [2012CB722605]

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beta-Alkoxy sulfides are widely used as versatile building blocks in organic synthesis. Therefore, it is highly desirable to develop a convenient and efficient method for oxysulfenylation of alkenes. In this communication, an easy and efficient metal-free approach to beta-alkoxy sulfides has been developed. The protocol uses readily available 1-(arylthio)pyrrolidine-2,5-diones and alcohols as the oxysulfenylating agents, chloroform as the solvent, and no ligand, additive and exclusion of air were required. Therefore, the present method provides a useful strategy for synthesis of beta-alkoxy sulfides.

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