期刊
JOURNAL OF FOOD SCIENCE
卷 77, 期 4, 页码 C408-C413出版社
WILEY
DOI: 10.1111/j.1750-3841.2011.02609.x
关键词
adsorptive transfer stripping voltammetry; antioxidant capacity; boron-doped diamond electrode; chlorogenic acid; coffee samples
In this study, an electroanalytical methodology for the determination of chlorogenic acid (CGA) was achieved at a boron-doped diamond electrode under adsorptive transfer stripping voltammetric conditions. The values obtained for CGA were used to estimate the antioxidant properties of the coffee sample based on CGA oxidation. By using square-wave stripping mode, the compound yielded a well-defined voltammetric response at +0.49 V with respect to Ag/AgCl in BrittonRobinson buffer at pH 3.0 (after 120 s accumulations at a fixed potential of 0.40 V). At the optimum experimental conditions, linear calibration curve is obtained within the concentration range of 0.25 to 4.0 mu g mL-1 with the limit of detection 0.049 mu g mL-1. The developed protocol was successfully applied for the analysis of antioxidant capacity in the coffee products such as Turkish coffee and instant coffee.
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