期刊
JOURNAL OF FLUORINE CHEMISTRY
卷 156, 期 -, 页码 307-313出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2013.07.012
关键词
Radical addition; Sulfide; Tetrafluoroethyl; Tetrafluoroethylene
资金
- Academy of Sciences of the Czech Republic [RVO: 61388963]
- Grant Agency of the Czech Republic [207/11/0421]
PhSCF2CF2Br in the presence of tributyltin hydride and substochiometric triethylborane in dichloromethane underwent radical addition to alkenes to give the bromine-free products. Reductive substitution of the phenylsulfanyl group for hydrogen in these adducts provided compounds with the tetrafluoroethyl group. Under the same conditions and in the presence of alkenes, radical addition took place to furnish tetrafluoroethylene-containing alkanes. (C) 2013 Elsevier B.V. All rights reserved.
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