期刊
JOURNAL OF FLUORINE CHEMISTRY
卷 139, 期 -, 页码 23-27出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2012.03.016
关键词
Fluorination; DAST; Phosphonates; Aminophophonates; Aziridinium ion
资金
- Wroclaw Research Centre EIT+ [POIG.01.01.02-02-003/08]
- European Regional Development Fund (Operational Programme Innovative Economy) [1.1.2]
Herein, we report a new and convenient method for the synthesis of beta-fluoro-alpha-aminophosphonates starting from naturally occurring L-amino acids. A key step in the synthetic protocol involves nucleophilic fluorination of N,N-dibenzylated-beta-amino alcohols with diethylaminosulfur trifluoride (DAST). (C) 2012 Elsevier B.V. All rights reserved.
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