期刊
JOURNAL OF FLUORINE CHEMISTRY
卷 131, 期 12, 页码 1353-1355出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2010.09.006
关键词
MgF2; Microemulsion; Chemical synthesis; Nanocrystalline; Inorganic materials
资金
- Bavarian Science Foundation (BFS) [PDOK-61-08]
- FORGLAS project
Nanosized MgF2 was synthesized by precipitation in microemulsions of water in cyclohexane stabilized by polyethylene glycol tert-octylphenyl ether. The synthesized MgF2 powder was characterized by transmission electron microscopy (TEM), scanning electron microscopy (SEM), BET specific surface area, attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR), and X-ray diffraction (XRD). The results showed that the synthesized powder was a MgF2 powder with a crystallite size in the range of 9-11 nm and a specific surface area of 190 m(2)/g. (C) 2010 Elsevier B.V. All rights reserved.
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