期刊
JOURNAL OF FLUORINE CHEMISTRY
卷 131, 期 11, 页码 1192-1197出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2010.06.009
关键词
Monofluoroolefination; Monofluoroalkenes; Monofluoromethyl arylsulfone; Julia-Kocienski reaction
资金
- Loker Hydrocarbon Research Institute
Monofluoromethyl 3 5-bis(trifluoromethyl)phenyl sulfone 1 was synthesized and employed in Julia-Kocienski fluoroolefination reaction with various ketones and aldehydes Optimal reaction conditions were found to be the treatment of substrates with KOH or CsF in DMSO at room temperature Mixtures of (E) and (Z) isomers of monofluoroalkenes 4 were obtained in moderate to excellent yields (C) 2010 Elsevier B V All rights reserved
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