期刊
JOURNAL OF FLUORINE CHEMISTRY
卷 130, 期 4, 页码 406-409出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2009.01.002
关键词
Ytterbium perfluorooctanoate; Doebner reaction; Pyruvic acid; Quinoline-4-caboxylic acid derivatives; One-pot reaction
资金
- National Nature Science Foundation of China [20672035]
- Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences
Ytterbium perfluorooctanoate [Yb(PFO)(3)] has been proved to be an efficient catalyst for Doebner reaction of pyruvic acid, aldehydes and amines under mild conditions in water to afford quinoline-4-caboxylic acid derivatives with three component one-pot method in good yields. The process is operationally simple and environmentally benign and the catalyst has readily been recycled for several times with consistent activity. Furthermore, a plausible mechanism for this transformation is also presented. (C) 2009 Elsevier B.V. All rights reserved.
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